take that, BaranIt took a hell of a lot longer to get here than I had planned, but now I should be able to make dozens of targets and their enantiomers without ever having to repeat any of those steps again.
Wednesday, July 1, 2009
gram scale
It took me a few months longer than I would have liked, but I finally got there. Here are two large (if I do say so myself) bottles of >99% ee enantiomers of my branching point compound. There should be more than 100 g of each, and there is a bit more coming through the resolution still. This is the culmination of seven steps and one resolution.
take that, Baran
It took a hell of a lot longer to get here than I had planned, but now I should be able to make dozens of targets and their enantiomers without ever having to repeat any of those steps again.
take that, BaranIt took a hell of a lot longer to get here than I had planned, but now I should be able to make dozens of targets and their enantiomers without ever having to repeat any of those steps again.
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2 comments:
Your TLC is ready
Iodine, bitches!
It's quick, very general, cheap, and not nearly as messy as a spray or even a dip. If you forget the plate in the tank for a few days and it's not readable, a little airing out usually does the trick.
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